Semiquantitative emission spectrographic analyses for 31 elements on 271 stream sediments and 53 rock samples from Sipsey Wilderness and additions, Lawrence and Winston Counties, Ala., are reported here in detail. All sample localities are given in Universal Transverse Mercator (UTM) coordinates. Brief descriptions of rock samples are also included. Rocks analyzed are mostly sandstone, shale, and limestone. No obviously anomalous values related to mineralized rock are in the data.