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Publications

Below are publication products associated with the Brine Research Instrumentation and Experimental (BRInE) Laboratory:

Dissolved organic matter within oil and gas associated wastewaters from U.S. unconventional petroleum plays: Comparisons and consequences for disposal and reuse

Wastewater generated during petroleum extraction (produced water) may contain high concentrations of dissolved organics due to their intimate association with organic-rich source rocks, expelled petroleum, and organic additives to fluids used for hydraulic fracturing of unconventional (e.g., shale) reservoirs. Dissolved organic matter (DOM) within produced water represents a challenge for treatmen
Authors
Bonnie McDevitt, Aaron M. Jubb, Matthew S. Varonka, Madalyn S. Blondes, Mark A Engle, Tanya J. Gallegos, Jenna L. Shelton

Insights on geochemical, isotopic, and volumetric compositions of produced water from hydraulically fractured Williston Basin oil wells

Tracing produced water origins from wells hydraulically fractured with freshwater-based fluids is sometimes predicated on assumptions that (1) each geological formation contains compositionally unique brine and (2) produced water from recently hydraulically fractured wells resembles fresher meteoric water more so than produced water from older wells. These assumptions are not valid in Williston Ba

Authors
Tanya J. Gallegos, Colin A. Doolan, Rodney R. Caldwell, Mark A Engle, Matthew S. Varonka, Justin E. Birdwell, Glenn D. Jolly, Tyler B. Coplen, Thomas A. Oliver

Utica shale play oil and gas brines: Geochemistry and factors influencing wastewater management

The Utica and Marcellus Shale Plays in the Appalachian Basin are the fourth and first largest natural gas producing plays in the United States, respectively. Hydrocarbon production generates large volumes of brine (“produced water”) that must be disposed of, treated, or reused. Though Marcellus brines have been studied extensively, there are few studies from the Utica Shale Play. This study presen

Authors
Madalyn S. Blondes, Jenna L. Shelton, Mark A Engle, Jason Trembly, Colin A. Doolan, Aaron M. Jubb, Jessica Chenault, Elisabeth L. Rowan, Ralph J. Haefner, Brian E. Mailot

Repetitive sampling and control threshold improve 16S rRNA results from produced waters associated with hydraulically fractured shales

Sequencing microbial DNA from deep subsurface environments is complicated by a number of issues ranging from contamination to non-reproducible results. Many samples obtained from these environments - which are of great interest due to the potential to stimulate microbial methane generation - contain low biomass. Therefore, samples from these environments are difficult to study as sequencing result
Authors
Jenna L. Shelton, Elliott Barnhart, Leslie F. Ruppert, Aaron M. Jubb, Madalyn S. Blondes, Christina A. DeVera

Origin and geochemistry of formation waters from the lower Eagle Ford Group, Gulf Coast Basin, south central Texas

The lower Eagle Ford Group (LEFG) is one of the most productive continuous hydrocarbon plays in the United States but few associated produced waters data and minimal interpretation have been published. This effort focuses on results from compositional and isotopic data from 39 produced water samples collected from horizontal wells producing from the LEFG in south central Texas. The depth of the LE
Authors
Mark A Engle, Colin A. Doolan, Janet K. Pitman, Matthew S. Varonka, Jessica Chenault, William H. Orem, Peter B. McMahon, Aaron M. Jubb

Organic compounds in produced waters from the Bakken Formation and Three Forks Formation in the Williston Basin, North Dakota

The organic composition of produced waters (flowback and formation waters) from the middle member of the Bakken Formation and the Three Forks Formation in the Williston Basin, North Dakota were examined to aid in the remediation of surface contamination and help develop treatment methods for produced-water recycling. Twelve produced water samples were collected from the Bakken and Three Forks Form
Authors
Matthew S. Varonka, Tanya Gallegos, Anne L. Bates, Colin A. Doolan, William H. Orem

Direct trace element determination in oil and gas produced waters with inductively coupled plasma - Optical emission spectrometry (ICP-OES): Advantages of high salinity tolerance

Waters co-produced during petroleum extraction are the largest waste stream from oil and gas development. Reuse or disposal of these waters is difficult due to their high salinities and the sheer volumes generated. Produced waters may also contain valuable mineral commodities. While an understanding of produced water trace element composition is required for evaluating the associated resource and
Authors
Aaron M. Jubb, Mark Engle, Jessica Chenault, Madalyn Blondes, Cloelle G. Danforth, Colin Doolan, Tanya Gallegos, Dan Mueller, Jenna Shelton

Accuracy of methods for reporting inorganic element concentrations and radioactivity in oil and gas wastewaters from the Appalachian Basin, U.S. based on an inter-laboratory comparison.

Accurate and precise analyses of oil and gas (O&G) wastewaters and solids (e.g., sediments and sludge) are important for the regulatory monitoring of O&G development and tracing potential O&G contamination in the environment. In this study, 15 laboratories participated in an inter-laboratory comparison on the chemical characterization of three O&G wastewaters from the Appalachian Basin and four so
Authors
Travis L. Tasker, William D Burgos, Moses A Ajemigbitse, Nancy E. Lauer, Alen V Gusa, Maksat Kuatbek, Dustin May, Joshua D. Landis, Daniel S. Alessi, Amanda M Johnsen, James M Kaste, Kurt Headrick, Franziska DH Wilke, Mark McNeal, Mark A. Engle, Aaron M. Jubb, Radisav Vidic, Avner Vengosh, Nathaniel R. Warner

Geochemistry of formation waters from the Wolfcamp and “Cline” shales: Insights into brine origin, reservoir connectivity, and fluid flow in the Permian Basin, USA

Despite being one of the most important oil producing provinces in the United States, information on basinal hydrogeology and fluid flow in the Permian Basin of Texas and New Mexico is lacking. The source and geochemistry of brines from the basin were investigated (Ordovician- to Guadalupian-age reservoirs) by combining previously published data from conventional reservoirs with geochemical resul
Authors
Mark A. Engle, Francisco R. Reyes, Matthew S. Varonka, William H. Orem, Ma Lin, Adam J. Ianno, Tiffani M. Westphal, Pei Xu, Kenneth C. Carroll
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